The TGA excess weight improve curve is proven in Determine 1. The primary fat loss step could be the volatilization followed by A serious decomposition stage. The by-product of bodyweight change curve in eco-friendly reveals a peak in which the height max is at 427.71 ˚C. The MS details is gathered throughout the total TGA experiment. Ion currents and TGA mass decline are plotted as being a purpose of temperature (see Figure two). It is important to bear in mind the goods of a TGA take a look at are Typically decomposition products, and that is real in these experiments in addition. Consequently, the intention is to know the thermal degradation solutions of nylon sixty six. TGA-MS constantly screens the decomposition off gases for a function of your time and temperature. The degradation system from the polymer molecules breaking with the C-N bond makes smaller polymer molecules With all the similar unit of bicarbonyl polymethylene fragments and also the fragments will stop working into carbon dioxide, carbon monoxide, water, and hydrocarbons [5].
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The degradation of nylon 66 On this A part tga66 of the study was also performed with a TGA5500. The off-gasoline items had been analyzed using a FTIR with the IR spectra in addition to a GC/MS to the MS Evaluation.
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